By Krzysztof Matyjaszewski (Eds.)
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25) Oberthur, R. C. Makromol. Chemie 1978, 179, 2693-2706. ; Kanaya, T. Polymer 2006, 47, 5669-5677. (27) Bovey, F. A. Chain Structure and Conformation of Macromolecules; Academic Press: New York, 1982. ; Lagally, P. Makromol. Chem. 1948, 1, 169-198. ; Ruckenstein, E. J. Appl. Polym. Sci. 1993, 49, 2179-2188. ; ACS Symposium Series; American Chemical Society: Washington, DC, 2009. ch003 Chapter 3 RAFT Polymerization of Vinyl Acetate, Styrene and Acrylates Using N,N-Dithiocarbamates Vidyasagar Malepu, Christy D.
The effect of initiator was more clearly seen in Figure 1C, which showed the PDI vs conversion profiles. As the initiator concentration was increased, the evolution of the PDI with conversion also increased. 6 for the highest [I] at high conversion. (5) The change in MWD as a function of conversion for Expts 1, 3, and 5 are shown in Figure 2, illustrating the influence of initiator concentration. In the presence of low concentrations of initiator (Expt 1, Figure 2A), the MWDs were narrow but with a low molecular weight shoulder at half the molecular weight of the main peak, becoming more predominant especially at high conversions.
Note: at high conversions, a second low molecular weight peak appears corresponding to the formation of the monofunctional RAFT agent species (refer to text). ; ACS Symposium Series; American Chemical Society: Washington, DC, 2009. 0 log i Figure 3. log 〈kt〉 vs. 15M) at 90°C, using 1,3-bis(benzyl-thiocarbonyl-sulfanyl-2-prop-2yl)benzene (BTBTPB, 50mM) and 1,1- azobis (cyclohexanecarbonitrile) (VAZO88) as initiator. The concentrations of VAZO88 used are approximately (a) 25mM, (b) 50mM, (c) 100mM, (d) 150mM, and (e) 200mM.